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Beilstein J. Org. Chem. 2014, 10, 2027–2037, doi:10.3762/bjoc.10.211
Graphical Abstract
Figure 1: The new charge-tagged proline-derived catalyst 1.
Scheme 1: Inverse aldol reaction with aldehyde donors according to Jørgensen [54]. We studied the reaction for R ...
Scheme 2: Synthesis of 4-(pyridin-4-yl)phenol (5).
Scheme 3: Synthesis of the charge-tagged proline catalyst 1.
Figure 2: Molecular structure of 7 in the solid state.
Scheme 4: Proposed catalytic cycle [36-38] for the aldol reaction with aldehyde donors [54]; CT = charge tag, a: R = Ph, ...
Figure 3: Experimental setup for continuous-flow ESIMS experiments using two mixing tee microreactors directl...
Figure 4: ESI mass spectra of acetonitrile solutions of diethyl ketomalonate and butyraldehyde (a) with unmod...
Figure 5: ESI(+) CID MS/MS spectra of mass-selected intermediates a) [IIb]+, b) the butyl ester derivative [I...
Figure 6: Normalized relative intensities in ESI spectra recorded for the inverse aldol reaction of butyralde...